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Various

"Scientific American Supplement, No. 832, December 12, 1891"

If the action is stopped before
all the silicon is consumed, the residue is found to be fused. As
crystalline silicon only melts at a temperature superior to 1,200 deg.,
the heat evolved must be very great. If the reaction is performed in
the fluorspar tube, the resulting gaseous silicon tetrafluoride,
SiF_{4}, may be collected over mercury.
Amorphous silicon likewise burns with great energy in fluorine.

ACTION OF FLUORINE UPON METALS.
_Sodium_ and _potassium_ combine with fluorine with great vigor at
ordinary temperatures, becoming incandescent, and forming their
respective fluorides, which may be obtained crystallized from water in
cubes. Metallic _calcium_ also burns in fluorine gas, forming the
fused fluoride, and occasionally minute crystals of fluorspar.
_Thallium_ is rapidly converted to fluoride at ordinary temperatures,
the temperature rising until the metal melts and finally becomes red
hot. Powdered _magnesium_ burns with great brilliancy. _Iron_, reduced
by hydrogen, combines in the cold with immediate incandescence, and
formation of an anhydrous, readily soluble, white fluoride.


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